C₁₃H₁₂Cl₃NO

Base Information

Chemical Name:C₁₃H₁₂Cl₃NO
CAS No.:1632314-58-9
Molecular Formula:C₁₃H₁₂Cl₃NO
Molecular Weight:304.603
Hs Code.:

C<sub>13</sub>H<sub>12</sub>Cl<sub>3</sub>NO

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₂Cl₃NO

Chemical Property:

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Technology Process of C₁₃H₁₂Cl₃NO

There total 4 articles about C₁₃H₁₂Cl₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620902-61-5
(2E)-3-(2-vinylphenyl)prop-2-en-1-ol

: 545-06-2
trichloroacetonitrile

: 1632314-58-9
C₁₃H₁₂Cl₃NO

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo5014492

Reference yield:

: 28272-96-0
2-vinylbenzaldehyde

: 1632314-58-9
C₁₃H₁₂Cl₃NO

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / hexane; diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide; In diethyl ether; hexane; dichloromethane; acetonitrile;
DOI:10.1021/jo5014492

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1632314-58-9
C₁₃H₁₂Cl₃NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / isopropyl alcohol / 18 h / 80 °C / Inert atmosphere

2.1: lithium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; lithium bromide; In diethyl ether; hexane; dichloromethane; isopropyl alcohol; acetonitrile; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo5014492