S-Phenyl 9-Hydroxydecanethioate

Base Information

Chemical Name:S-Phenyl 9-Hydroxydecanethioate
CAS No.:134781-57-0
Molecular Formula:C₁₆H₂₄O₂S
Molecular Weight:280.431
Hs Code.:

Synonyms:

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Chemical Property of S-Phenyl 9-Hydroxydecanethioate

Chemical Property:

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Technology Process of S-Phenyl 9-Hydroxydecanethioate

There total 5 articles about S-Phenyl 9-Hydroxydecanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25601-41-6
methyl 9-decenoate

: 134781-57-0
S-Phenyl 9-Hydroxydecanethioate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / KOH / H₂O; tetrahydrofuran / 14 h / Ambient temperature

2: 1) Hg(OAc)2, 2) 3M NaOH, NaBH₄ / 1) water/THF, 1h, rt 2) 3h, rt

3: 1) 2,2'-dipyridyl disulfide, Ph₃P / 1) benzene, 1h, rt, 2) 3h

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; 2,2'-dipyridyldisulphide; mercury(II) diacetate; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1021/jo00017a027

Reference yield:

: 50530-12-6
10-bromodecanoic acid

: 134781-57-0
S-Phenyl 9-Hydroxydecanethioate

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / TsOH / 24 h / Ambient temperature

2: 1) o-Nitrophenyl selenocyanate, NaBH₄ 2) 30percent H₂O₂ / 1) EtOH, THF, 8h, RT 2) 6h, RT

3: 90 percent / KOH / H₂O; tetrahydrofuran / 14 h / Ambient temperature

4: 1) Hg(OAc)2, 2) 3M NaOH, NaBH₄ / 1) water/THF, 1h, rt 2) 3h, rt

5: 1) 2,2'-dipyridyl disulfide, Ph₃P / 1) benzene, 1h, rt, 2) 3h

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; 2,2'-dipyridyldisulphide; mercury(II) diacetate; dihydrogen peroxide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1021/jo00017a027

Reference yield:

: 26825-94-5
10-bromodecanoic acid methyl ester

: 134781-57-0
S-Phenyl 9-Hydroxydecanethioate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) o-Nitrophenyl selenocyanate, NaBH₄ 2) 30percent H₂O₂ / 1) EtOH, THF, 8h, RT 2) 6h, RT

2: 90 percent / KOH / H₂O; tetrahydrofuran / 14 h / Ambient temperature

3: 1) Hg(OAc)2, 2) 3M NaOH, NaBH₄ / 1) water/THF, 1h, rt 2) 3h, rt

4: 1) 2,2'-dipyridyl disulfide, Ph₃P / 1) benzene, 1h, rt, 2) 3h

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; 2,2'-dipyridyldisulphide; mercury(II) diacetate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1021/jo00017a027