1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol)

Base Information

Chemical Name:1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol)
CAS No.:101083-14-1
Molecular Formula:C15H28O2
Molecular Weight:240.386
Hs Code.:
DSSTox Substance ID:DTXSID40579063
Nikkaji Number:J803.719A
Wikidata:Q82469468
Mol file:101083-14-1.mol

Synonyms:101083-14-1;1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol);SCHEMBL596112;DTXSID40579063

Suppliers and Price of 1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol)

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:240.208930132
Heavy Atom Count:17
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)(CCCC2(CCCCC2)O)O

Technology Process of 1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol)

There total 12 articles about 1,1'-(Propane-1,3-diyl)di(cyclohexan-1-ol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3384-04-1
3-chloropropyl phenyl ether

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 6963-45-7
1-(3-hydroxypropyl)-cyclohexanol

: 101083-14-1
1-[3-(1-hydroxycyclohexyl)propyl]cyclohexanol

Guidance literature:: 3-chloropropyl phenyl ether; With di(tert-butyl)-biphenyl; lithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

cyclohexanone; at 20 ℃; for 1.5h;

cyclohexanone; at -78 ℃; for 0.0833333h; Further stages.;
DOI:10.1021/jo000039m

Reference yield: 66.0%

: 28118-53-8
1,3-bis(phenylthio)propane

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 101083-14-1
1-[3-(1-hydroxycyclohexyl)propyl]cyclohexanol

Guidance literature:: 1,3-bis(phenylthio)propane; With 4,4'-di-tert-butylbiphenyl; lithium; In tetrahydrofuran; at -78 ℃; for 2h;

cyclohexanone; In tetrahydrofuran; at -78 ℃;

With water; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/S0040-4039(00)00764-4

Reference yield:

: 108-95-2,27073-41-2
phenol

: 101083-14-1
1-[3-(1-hydroxycyclohexyl)propyl]cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / KOH / methanol / 2 h / 60 °C

2.1: Li; di-tert-butylbiphenyl / tetrahydrofuran / 0.5 h / -78 °C

2.2: 1.5 h / 20 °C

2.3: 70 percent / 0.08 h / -78 °C

With potassium hydroxide; di(tert-butyl)-biphenyl; lithium; In tetrahydrofuran; methanol; 1.1: Etherification / 2.1: Metallation / 2.2: Addition / 2.3: Addition;
DOI:10.1021/jo000039m