cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

Base Information

Chemical Name:cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone
CAS No.:108672-56-6
Molecular Formula:C₁₄H₂₄N₂O₃
Molecular Weight:268.356
Hs Code.:

Synonyms:

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Chemical Property of cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

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Technology Process of cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

There total 1 articles about cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119-60-8
dicyclohexyl ketone

: 74-88-4
methyl iodide

: 108672-56-6
cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

Guidance literature:: With nitrogen(II) oxide; sodium methylate; Multistep reaction; 1) methanol, 65 deg C, 18 h, 2) methanol;

Reference yield:

: 108672-56-6
cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

: 108672-63-5
C₈H₁₄N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) nitric oxide, sodium methylate / 1.) MeOH, 40 deg C, 9 h, 2.) 60 deg C, 3 h

2: KOH / methanol / Heating

With potassium hydroxide; nitric oxide; sodium methylate; In methanol;

Reference yield:

: 108672-56-6
cyclohexyl-1-(2-methoxydiazene-1-oxide-1-yl)cyclohexyl ketone

: C₁₄H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) nitric oxide, sodium methylate / 1.) MeOH, 40 deg C, 9 h, 2.) 60 deg C, 3 h

2: 170 - 200 °C

With nitric oxide; sodium methylate;