[C₂₀H₈N₄(C₆H₅)3(C₆H₄OCO(CH₂)10CH₃)]YbOH

Base Information

• Chemical Name: [C₂₀H₈N₄(C₆H₅)3(C₆H₄OCO(CH₂)10CH₃)]YbOH
• CAS No.: 1006888-30-7
• Molecular Formula: C₅₆H₅₁N₄O₃Yb
• Molecular Weight: 1001.09
• Mol file: 1006888-30-7.mol

Synonyms:

Chemical Property of [C₂₀H₈N₄(C₆H₅)3(C₆H₄OCO(CH₂)10CH₃)]YbOH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [C₂₀H₈N₄(C₆H₅)3(C₆H₄OCO(CH₂)10CH₃)]YbOH

There total 1 articles about [C₂₀H₈N₄(C₆H₅)3(C₆H₄OCO(CH₂)10CH₃)]YbOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

ytterbium(III) chloride hexahydrate (10035-01-5) + [5-(p-dodecanoyl)phenyl-10,15,20-triphenyl]porphyrin → [C20H8N4(C6H5)3(C6H4OCO(CH2)10CH3)]YbOH (1006888-30-7)

Guidance literature:

In chloroform; water; mixt. heated in imidazole melt at 210 °C under protection and stirring of dry N2 stream for 2 h, cooling to 100 °C, distd. H2O added, soln. filtered, washed with distd. H2O, dried under vac.; dissolved in chloroform, shaken with 0.1% AgNO3, chloroform layer sepd.,mixt of chloroform and methanol added, shaken with aq. AgNO3-soln., con cd., chromd.; elem. anal.;

DOI:10.1016/j.jpcs.2007.01.018

upstream raw materials:

ytterbium(III) chloride hexahydrate