triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

Base Information

Chemical Name:triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide
CAS No.:109707-61-1
Molecular Formula:Br*C₃₀H₃₂OP
Molecular Weight:519.461
Hs Code.:

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Chemical Property of triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

Chemical Property:

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Technology Process of triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

There total 4 articles about triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107153-49-1
o-butoxyphenylethanol

: 109707-61-1
triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / PBr₃, pyridine / diethyl ether / 1.) -30 deg C, 1 h; 2.) 20 deg C, 3 h

2: 4.13 g / acetonitrile / 144 h / Heating; sealed glass tube

With pyridine; phosphorus tribromide; In diethyl ether; acetonitrile;

Reference yield:

: 28456-81-7
o-butoxyallylbenzene

: 109707-61-1
triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ozone-oxygen; 2.) sodium borohydride / 1.) methanol, 10 deg C; 2.) room temp.

2: 65 percent / PBr₃, pyridine / diethyl ether / 1.) -30 deg C, 1 h; 2.) 20 deg C, 3 h

3: 4.13 g / acetonitrile / 144 h / Heating; sealed glass tube

With pyridine; sodium tetrahydroborate; oxygen; phosphorus tribromide; ozone; In diethyl ether; acetonitrile;

Reference yield:

: 3383-08-2
3-(2-hydroxyphenyl)prop-1-ene sodium salt

: 109707-61-1
triphenyl-2-(o-butoxyphenyl)ethylphosphonium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / dimethylformamide / 6 h / 20 °C

2: 1.) ozone-oxygen; 2.) sodium borohydride / 1.) methanol, 10 deg C; 2.) room temp.

3: 65 percent / PBr₃, pyridine / diethyl ether / 1.) -30 deg C, 1 h; 2.) 20 deg C, 3 h

4: 4.13 g / acetonitrile / 144 h / Heating; sealed glass tube

With pyridine; sodium tetrahydroborate; oxygen; phosphorus tribromide; ozone; In diethyl ether; N,N-dimethyl-formamide; acetonitrile;