3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

Base Information

Chemical Name:3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate
CAS No.:78501-61-8
Molecular Formula:C₂₁H₂₈O₆
Molecular Weight:376.45
Hs Code.:

Synonyms:

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Chemical Property of 3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

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Technology Process of 3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

There total 3 articles about 3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-04-9
Adipic acid

: 78501-61-8
3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

Guidance literature:: Multi-step reaction with 2 steps

1: 7.5 g / triethylamine / acetone / Ambient temperature

2: 5.3 g / CDI, DBN / benzene / 4 h / Ambient temperature

With 2,6-dichloro-benzonitrile; triethylamine; 1,1'-carbonyldiimidazole; In acetone; benzene;
DOI:10.1002/hlca.19810640132

Reference yield:

: 78501-56-1
3-methyl-1-(tetrahydro-2-pyranyloxy)-5-hexen-3-ol

: 78501-61-8
3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

Guidance literature:: Multi-step reaction with 2 steps

1: 16.0 g / p-toluenesulfonic acid / methanol / 1 h / Ambient temperature

2: 5.3 g / CDI, DBN / benzene / 4 h / Ambient temperature

With 2,6-dichloro-benzonitrile; toluene-4-sulfonic acid; 1,1'-carbonyldiimidazole; In methanol; benzene;
DOI:10.1002/hlca.19810640132

Reference yield:

: 70-11-1
α-bromoacetophenone

: 78501-61-8
3'-hydroxy-3'-methyl-5'-hexenyl phenacyl adipate

Guidance literature:: Multi-step reaction with 2 steps

1: 7.5 g / triethylamine / acetone / Ambient temperature

2: 5.3 g / CDI, DBN / benzene / 4 h / Ambient temperature

With 2,6-dichloro-benzonitrile; triethylamine; 1,1'-carbonyldiimidazole; In acetone; benzene;
DOI:10.1002/hlca.19810640132