1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide

Base Information

• Chemical Name: 1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide
• CAS No.: 1000886-19-0
• Molecular Formula: C₁₃H₁₉N₄O₂S*Cl
• Molecular Weight: 330.838
• Mol file: 1000886-19-0.mol

Synonyms:

Chemical Property of 1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide

There total 1 articles about 1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.6%

girard's reagent T (123-46-6) + Benzoyl isothiocyanate (532-55-8) → 1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide (1000886-19-0)

Guidance literature:

In ethanol; for 4h; Heating;

DOI:10.1016/j.molstruc.2007.01.054

Reference yield:

1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide (1000886-19-0) + nickel(II) acetate hydrate → [Ni(1-acetyl trimethylammonium chloride-4-benzoyl thiosemicarbazide(-2H))(H2O)3]*2H2O

Guidance literature:

In ethanol; ligand and Ni salt in EtOH refluxed for 2-3 h; filtered while hot; ppt. washed with EtOH and Et2O; dried in vac. over CaCl2; elem. anal.;

DOI:10.1016/j.molstruc.2007.01.054

upstream raw materials:

girard's reagent T

Benzoyl isothiocyanate