p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane

Base Information

Chemical Name:p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane
CAS No.:1404110-95-7
Molecular Formula:C₃₀H₂₃ISi
Molecular Weight:538.503
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane

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Technology Process of p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane

There total 1 articles about p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1714-29-0
1-bromopyrene

: 146748-21-2
bis(4-iodophenyl)dimethylsilane

: 1404110-95-7
p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane

Guidance literature:: 1-bromopyrene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With ZnCl₂-TMEDA; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

bis(4-iodophenyl)dimethylsilane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 48.5h; Inert atmosphere;
DOI:10.1021/ol302742g

Reference yield:

: 1404110-95-7
p-iodophenyl-p-(1-pyrenyl)phenyldimethylsilane

: 1404110-91-3
C₆₁H₅₃BN₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; copper(ll) sulfate pentahydrate / dodecane / 72 h / 220 °C / Inert atmosphere; Schlenk technique

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -100 °C / Inert atmosphere

2.2: 17 h / -100 - 20 °C / Inert atmosphere

With n-butyllithium; copper(ll) sulfate pentahydrate; potassium carbonate; In tetrahydrofuran; dodecane; hexane; 1.1: |Ullmann Condensation;
DOI:10.1021/ol302742g