Os₂Cl₂(C₆H₅CONH)4

Base Information

Chemical Name:Os₂Cl₂(C₆H₅CONH)4
CAS No.:93121-30-3
Molecular Formula:C₂₈H₂₄Cl₂N₄O₄Os₂
Molecular Weight:931.829
Hs Code.:

Os<sub>2</sub>Cl<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>CONH)4

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os₂Cl₂(C₆H₅CONH)4

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Technology Process of Os₂Cl₂(C₆H₅CONH)4

There total 1 articles about Os₂Cl₂(C₆H₅CONH)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 81519-41-7
[Os(III)2(acetoxy)4Cl₂]

: 55-21-0,27208-38-4
benzamide

: 93121-30-3
Os₂Cl₂(C₆H₅CONH)4

Guidance literature:: In neat (no solvent); Os-complex was mixed with excess of benzamide under N2, immersed in oil bath, heated with stirring at 140-150°C for 72 h; sublimed at 140°C under high vac., washed with benzene and Et2O, recrystd. by slow diffusion of MeOH (containing Et4NCl) into Me2SO soln. of the product; elem. anal.;

Reference yield: 30.0%

: 93121-30-3
Os₂Cl₂(C₆H₅CONH)4

: 64-20-0
tetramethylammonium bromide

: 95482-46-5
Os₂Br₂(C₆H₅CONH)4

Guidance literature:: In methanol; dimethyl sulfoxide; soln. of Os-complex in Me2SO was filtered, soln. of Me4NBr in MeOH was slowly added on the top of Me2SO soln.; crystd. by slow diffusion of solvents;