2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

Base Information

Chemical Name:2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane
CAS No.:444082-87-5
Molecular Formula:C₆₀H₁₃₄Sb₂SeSi₁₄
Molecular Weight:1571.38
Hs Code.:

Synonyms:

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Chemical Property of 2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

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Technology Process of 2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

There total 3 articles about 2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 212389-19-0
2,4,6-tris[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]-1,3,5,2,4,6-triselenatristibane

: 7732-18-5
water

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: (((CH₃)3Si)2CH)2((CH₃)3Si)3CC₆H₂SbC₄H₄(CH₃)2*0.5H₂O

: 444082-87-5,212389-17-8
2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

Guidance literature:: With P(N(CH₃)2)3; In toluene; a toluene soln. was heated at 130°C in a sealed tube for 38 h (Ar); GPLC; elem. anal.;
DOI:10.1246/bcsj.75.661

Reference yield: 50.0%

: 7782-49-2
selenium

: 371165-49-0,212389-20-3
1,2-bis{2,6-bis[bis(trimethylsilyl)methyl]-4-[tris-(trimethylsilyl)methyl]phenyl}distibene

: 444082-87-5,212389-17-8
2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

Guidance literature:: With Et₃N; In benzene-d6; (Ar); Se (3 equiv.) and Et3N (3 equiv.) were added to soln. of Sb compd.in C6D6; degassed; sealed in NMR tube; heated at 60°C for 4 d; recrystd. (hexane);
DOI:10.1246/bcsj.80.2425

Reference yield: 33.0%

: 212389-19-0
2,4,6-tris[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]-1,3,5,2,4,6-triselenatristibane

: 444082-87-5,212389-17-8
2,3-bis[2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl]selenadistibirane

: 371165-49-0,212389-20-3
(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)Sb=Sb(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)

Guidance literature:: With P(N(CH₃)2)3; In ⁽²⁾H₈-toluene; to a toluene soln. of Sb-compound was added P(N(CH3)2)3, the mixt. was heated at 130°C in a sealed tube for 33 h, the mixt. was cooled toroom temp. (Ar); filtered; elem. anal.;
DOI:10.1246/bcsj.75.661