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Technology Process of C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6

C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6

Base Information
  • Chemical Name:C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6
  • CAS No.:522652-75-1
  • Molecular Formula:C38H45ClIr2N2PS2*F6P
  • Molecular Weight:1189.75
  • Hs Code.:
C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub><sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub>]PF<sub>6</sub>

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Chemical Property of C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6
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Technology Process of C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6

There total 2 articles about C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

silver(I) hexafluorophosphate
26042-63-7

silver(I) hexafluorophosphate

IrCl2(pentamethylcyclopentadienyl)PPh3

IrCl2(pentamethylcyclopentadienyl)PPh3

5-(η5-pentamethylcyclopentadienyl)d-5,1,3,2,4-iridiadithiadiazole
522652-73-9

5-(η5-pentamethylcyclopentadienyl)d-5,1,3,2,4-iridiadithiadiazole

C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub><sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub>]PF<sub>6</sub>
522652-75-1

C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6

Guidance literature:
In dichloromethane; byproducts: AgCl; (N2 or Ar); addn. of silver salt to a soln. of iridium complex in CH2Cl2, stirring for 2 h in the dark, addn. of tin complex, addn. of CH2Cl2, stirring for 2 h at room temp. in the dark; filtration through Celite, concn., addn. of Et2O, filtration, washing with Et2O, drying in vac.; elem. anal.;
DOI:10.1139/v02-085

Reference yield: 37.0%

ammonium hexafluorophosphate

ammonium hexafluorophosphate

IrCl2(pentamethylcyclopentadienyl)PPh3

IrCl2(pentamethylcyclopentadienyl)PPh3

[(n-butyl)2Sn(S<sub>2</sub>N<sub>2</sub>)]2
369632-12-2

[(n-butyl)2Sn(S2N2)]2

C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub><sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[C<sub>5</sub>(CH<sub>3</sub>)5IrClP(C<sub>6</sub>H<sub>5</sub>)3C<sub>5</sub>(CH<sub>3</sub>)5IrS<sub>2</sub>N<sub>2</sub>]PF<sub>6</sub>
522652-75-1

C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2(1+)*PF6(1-)=[C5(CH3)5IrClP(C6H5)3C5(CH3)5IrS2N2]PF6

Guidance literature:
In dichloromethane; (N2 or Ar); addn. of tin complex and ammonium salt to a soln. of iridiumcomplex in CH2Cl2, stirring for 18 h at room temp.; filtration through Celite, evapn., slow concn. over 2 wk, sepn., washingwith Et2O, drying in vac.;
DOI:10.1139/v02-085
upstream raw materials:

[(n-butyl)2Sn(S2N2)]2

silver(I) hexafluorophosphate

5-(η5-pentamethylcyclopentadienyl)d-5,1,3,2,4-iridiadithiadiazole

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