Technology Process of C29H33N5O
There total 5 articles about C29H33N5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
butan-1-ol;
at 150 ℃;
for 0.166667h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2014.12.050
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
2: tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate; caesium carbonate / 1,4-dioxane / 90 °C
3: trifluoroacetic acid / dichloromethane / 20 °C
4: hydrazine hydrate / butan-1-ol / 0.17 h / 150 °C / Microwave irradiation
With
tris-(dibenzylideneacetone)dipalladium(0); benzotriazol-1-ol; caesium carbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; tri tert-butylphosphoniumtetrafluoroborate;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2014.12.050
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
2: tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate; caesium carbonate / 1,4-dioxane / 90 °C
3: trifluoroacetic acid / dichloromethane / 20 °C
4: hydrazine hydrate / butan-1-ol / 0.17 h / 150 °C / Microwave irradiation
With
tris-(dibenzylideneacetone)dipalladium(0); benzotriazol-1-ol; caesium carbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; tri tert-butylphosphoniumtetrafluoroborate;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2014.12.050
