PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

Base Information

Chemical Name:PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4
CAS No.:72883-68-2
Molecular Formula:C₂₅H₃₂O₄P₂W
Molecular Weight:642.324
Hs Code.:

PH(C<sub>6</sub>H<sub>5</sub>)2WP(CH(CH<sub>3</sub>)2)3(CO)4

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Chemical Property of PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

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Technology Process of PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

There total 2 articles about PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 80227-30-1,64654-54-2
tetraethylammonium chlorotetracarbonyltriisopropylphosphinewolframate

: 829-85-6
diphenylphosphane

: 72883-68-2,72904-55-3
PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

Guidance literature:: In ethanol; (N2); soln. of W complex and phosphine was stirred for 6 h at 20°C; after some h formed ppt. was filtered off, washed with EtOH and recrystd. from toluene/PE; elem. anal.;
DOI:10.1016/S0022-328X(00)83486-5

Reference yield: 64.0%

: 72883-68-2,72904-55-3
PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

: 72883-68-2,72904-55-3
PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

Guidance literature:: In methyl cyclohexane; (N2); soln. of W complex was heated at 80°C for 2 h, cooled to 20°C and seed crystals of cis-isomer were added; after standing overnight at 0°C cis-isomer was filtered off, solvent was removed in vac., residue recrystd. from CH2Cl2/EtOH; elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(00)83486-5

Reference yield: 64.0%

: 72883-68-2,72904-55-3
PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

: 72883-68-2,72904-55-3
PH(C₆H₅)2WP(CH(CH₃)2)3(CO)4

Guidance literature:: In methyl cyclohexane; (N2); soln. of W complex was heated at 80°C for 2 h, cooled to 20°C and seed crystals of cis-isomer were added; after standing overnight at 0°C cis-isomer was filtered off, solvent was removed in vac., residue recrystd. from CH2Cl2/EtOH; elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(00)83486-5