methoxy(phenyl)methyl-o-carborane

Base Information

Chemical Name:methoxy(phenyl)methyl-o-carborane
CAS No.:257889-17-1
Molecular Formula:C₁₀H₂₀B₁₀O
Molecular Weight:264.378
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxy(phenyl)methyl-o-carborane

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Technology Process of methoxy(phenyl)methyl-o-carborane

There total 1 articles about methoxy(phenyl)methyl-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 20539-32-6,257889-14-8
1-(o-carboranyl)benzyl alcohol

: 74-88-4
methyl iodide

: 257889-10-4,257889-17-1
methoxy(phenyl)methyl-o-carborane

Guidance literature:: 1-(o-carboranyl)benzyl alcohol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.jorganchem.2009.10.030

Reference yield: 83.0%

: 257889-10-4,257889-17-1
methoxy(phenyl)methyl-o-carborane

: 2767-47-7
dimethyltin dibromide

: [methoxy(phenyl)methyl-o-carboranyl]SnMe₂Br

Guidance literature:: With n-butyllithium; In diethyl ether; under inert gas; soln. of N-BuLi (3.3 mmol) added to stirred soln. of methoxy(phenyl)methyl-o-carborane (3.0 mmol) in Et2O at -10°C, stirred for 30 min, soln. of Me2SnBr(3.0 mmol) in Et2O added at -10°C, allowed to stand for 10 min; filtered, solvent removed, residue dissolved in toluene, concd., allowedto stand at -10°C for 2 d for crystn.; elem. anal.;
DOI:10.1016/j.jorganchem.2009.10.030