Anhydrogrevillin D

Base Information

Chemical Name:Anhydrogrevillin D
CAS No.:104555-21-7
Molecular Formula:C₁₈H₁₀O₇
Molecular Weight:338.273
Hs Code.:

Synonyms:

Suppliers and Price of Anhydrogrevillin D

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Anhydrogrevillin D

Chemical Property:

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Technology Process of Anhydrogrevillin D

There total 7 articles about Anhydrogrevillin D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 54707-49-2
Grevillin D

: 104555-21-7
Anhydrogrevillin D

Guidance literature:: With sulfuric acid; In methanol; for 31h; Heating;

Reference yield:

: 52711-92-9
2,5-dimethoxyphenylacetyl chloride

: 104555-21-7
Anhydrogrevillin D

Guidance literature:: Multi-step reaction with 6 steps

1: 2.) 48percent aq. sol. HBr / 1.) ether, 1 h, 20 deg C; 2.) 1 h, 20 deg C

2: 57 percent / H₂O; dimethylsulfoxide / 1.) 10 min, 50 deg C; 2.) 14 h, RT

3: 42 percent / potassium tert-butoxide / hexamethylphosphoric acid triamide / 60 h / 25 °C

4: 48 percent / conc. HCl / acetic acid / 2 h / 60 °C

5: 68 percent / BBr₃ / CH₂Cl₂ / 0.5 h / Heating

6: 41 percent / conc. H₂SO₄ / methanol / 31 h / Heating

With hydrogenchloride; sulfuric acid; potassium tert-butylate; hydrogen bromide; boron tribromide; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; acetic acid; dimethyl sulfoxide;

Reference yield:

: 104554-98-5
α-bromomethyl(2,5-dimethoxybenzyl)ketone

: 104555-21-7
Anhydrogrevillin D

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / H₂O; dimethylsulfoxide / 1.) 10 min, 50 deg C; 2.) 14 h, RT

2: 42 percent / potassium tert-butoxide / hexamethylphosphoric acid triamide / 60 h / 25 °C

3: 48 percent / conc. HCl / acetic acid / 2 h / 60 °C

4: 68 percent / BBr₃ / CH₂Cl₂ / 0.5 h / Heating

5: 41 percent / conc. H₂SO₄ / methanol / 31 h / Heating

With hydrogenchloride; sulfuric acid; potassium tert-butylate; boron tribromide; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; acetic acid; dimethyl sulfoxide;