2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide

Base Information

• Chemical Name: 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide
• CAS No.: 1356496-32-6
• Molecular Formula: C₁₈H₂₀N₄O₄S₂
• Molecular Weight: 420.513

Synonyms:

Chemical Property of 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide

Chemical Property:

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Technology Process of 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide

There total 5 articles about 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2-chloroethane-1-sulfonylazide (15980-09-3) + Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amine (148679-34-9) → 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide (1356496-32-6)

Guidance literature:

2-chloroethane-1-sulfonylazide; With potassium carbonate; Sealed tube;

With potassium iodide; Sealed tube;

Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amine; Sealed tube;

DOI:10.1007/s10593-019-02609-z

Reference yield:

2-(phenylthio)ethanamine (2014-75-7) → 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide (1356496-32-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium sulfate / tetrahydrofuran / 3 h / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / water; acetonitrile / 3 h / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; potassium iodide; In tetrahydrofuran; methanol; water; acetonitrile;

DOI:10.1039/c1cc14724b

Reference yield:

piperonal (120-57-0,30024-74-9) → 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonyl azide (1356496-32-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium sulfate / tetrahydrofuran / 3 h / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / water; acetonitrile / 3 h / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; potassium iodide; In tetrahydrofuran; methanol; water; acetonitrile;

DOI:10.1039/c1cc14724b

upstream raw materials:

piperonal

2-chloroethane-1-sulfonylazide

Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amine

2-(phenylthio)ethanamine

Downstream raw materials:

2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

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