2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

Base Information

Chemical Name:2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide
CAS No.:1356496-15-5
Molecular Formula:C₂₇H₃₀N₆O₇S₂
Molecular Weight:614.703
Hs Code.:

2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

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Chemical Property of 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

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Technology Process of 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

There total 6 articles about 2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2014-75-7
2-(phenylthio)ethanamine

: 1356496-15-5
2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium sulfate / tetrahydrofuran / 3 h / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / water; acetonitrile / 3 h / Inert atmosphere

4: N,N-dimethyl-formamide / 0.02 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; potassium iodide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c1cc14724b

Reference yield:

: 1356496-24-6
(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-thioacetic acid S-(9H-fluoren-9-ylmethyl) ester

: 1356496-15-5
2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.02 h / 20 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 0.02 h / 20 °C / Inert atmosphere

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1039/c1cc14724b

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1356496-15-5
2-[benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-amino]-ethanesulfonic acid [2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purin-7-yl)-acetyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium sulfate / tetrahydrofuran / 3 h / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / water; acetonitrile / 3 h / Inert atmosphere

4: N,N-dimethyl-formamide / 0.02 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; potassium iodide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c1cc14724b