trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium]

Base Information

• Chemical Name: trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium]
• CAS No.: 95189-91-6
• Molecular Formula: C₈H₁₂Cl₂Rh*C₅₅H₅₅ClN₂OP₂PtRh
• Molecular Weight: 1437.44

Synonyms:

Chemical Property of trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium]

There total 2 articles about trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro(C(NC6H4OMe-p)COMe)bis(triphenylphosphine)platinum (78206-31-2,78419-44-0) → trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium] (95189-91-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₃NH₂ / not given

2: not given

With CH₃NH₂; In not given;

Reference yield:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) + trans-chloro-[1-(p-methoxyphenylimino)-2-(methylimino)propyl]bis(triphenylphosphine)platinum (88887-10-9) → trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt][dichloro(η4-cyclo-octa-1,5-diene)rhodium] (95189-91-6)

Guidance literature:

In not given; Pt complex mixed with Rh complex (molar ratio 1:1) in CDCl3 or MeOH; not isolated, detected by NMR;

upstream raw materials:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

trans-chloro-[1-(p-methoxyphenylimino)-2-(methylimino)propyl]bis(triphenylphosphine)platinum

chloro(C(NC₆H₄OMe-p)COMe)bis(triphenylphosphine)platinum

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