trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

Base Information

Chemical Name:trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate
CAS No.:131704-05-7
Molecular Formula:C₂H₂O₄*C₁₉H₂₃NO₂
Molecular Weight:387.433
Hs Code.:

Synonyms:

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Chemical Property of trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

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Technology Process of trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

There total 4 articles about trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 58574-67-7,122431-56-5,122431-61-2
trans-2-((dimethylamino)methyl)-2,3-dihydroinden-1-ol

: 150-76-5
4-methoxy-phenol

: 131704-00-2,131704-05-7
cis-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

: 131704-00-2,131704-05-7
trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In benzene; below 35 deg C;
DOI:10.1021/jo00002a033

Reference yield: 12.0%

: 58574-67-7,122431-56-5,122431-61-2
trans-2-((dimethylamino)methyl)-2,3-dihydroinden-1-ol

: 150-76-5
4-methoxy-phenol

: 131704-00-2,131704-05-7
cis-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

: 131704-00-2,131704-05-7
trans-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In benzene; below 35 deg C;
DOI:10.1021/jo00002a033

Reference yield:

: 16931-84-3
2-((dimethylamino)methyl)-2,3-dihydro-1H-inden-1-one hydrochloride

: 131704-00-2,131704-05-7
cis-N,N-dimethyl-2,3-dihydro-1-(4-methoxyphenoxy)indene-2-methanamine oxalate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / NaBH₄ / H₂O / 5 h / 0 °C

2: 20 percent / Ph₃P, diethyl azodicarboxylate / benzene / below 35 deg C

With sodium tetrahydroborate; triphenylphosphine; diethylazodicarboxylate; In water; benzene;
DOI:10.1021/jo00002a033