benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

Base Information

Chemical Name:benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide
CAS No.:111196-03-3
Molecular Formula:C₂₃H₂₇N₅O₇
Molecular Weight:485.497
Hs Code.:

Synonyms:

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Chemical Property of benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

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Technology Process of benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

There total 3 articles about benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 111196-03-3
benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / N-ethylpiperidine, N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 1) -5 deg C; 2) 0 deg C, 2 h; 3) 12h, room temp.

2: 84 percent / 80percent hydrazine hydrate / methanol / 24 h / Ambient temperature

3: 1) NaNO₂, 20percent HCl / 1) water, ethyl acetate, THF, -10 deg C, 8 min.; 2) DMF, 12 h, 3 deg C

With 1-ethyl-piperidine; hydrogenchloride; hydrazine hydrate; dicyclohexyl-carbodiimide; sodium nitrite; In methanol; dichloromethane;

Reference yield:

: 65005-45-0
benzyloxycarbonylalanyl-β-alanine ethyl ester

: 111196-03-3
benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 80percent hydrazine hydrate / methanol / 24 h / Ambient temperature

2: 1) NaNO₂, 20percent HCl / 1) water, ethyl acetate, THF, -10 deg C, 8 min.; 2) DMF, 12 h, 3 deg C

With hydrogenchloride; hydrazine hydrate; sodium nitrite; In methanol;

Reference yield:

: 1668-13-9,26017-82-3,26432-41-7,77286-89-6
L-alanine-p-nitroanilide

: 82938-87-2
N-(N-benzyloxycarbonyl-L-alanyl)-β-alanine hydrazide

: 111196-03-3
benzyloxycarbonylalanyl-β-alanyl-alanine p-nitroanilide

Guidance literature:: With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1) water, ethyl acetate, THF, -10 deg C, 8 min.; 2) DMF, 12 h, 3 deg C;