C₄₂H₄₆N₂O₈Si

Base Information

Chemical Name:C₄₂H₄₆N₂O₈Si
CAS No.:1453217-83-8
Molecular Formula:C₄₂H₄₆N₂O₈Si
Molecular Weight:734.921
Hs Code.:

C<sub>42</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>Si

Synonyms:

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Chemical Property of C₄₂H₄₆N₂O₈Si

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Technology Process of C₄₂H₄₆N₂O₈Si

There total 7 articles about C₄₂H₄₆N₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1453217-80-5
1-(2,5-O-diacetyl-3-O-(2-naphthylmethyl)-4-C-(tert-butyldiphenylsilyl)oxymethyl-6-deoxy-6-C-vinyl-α-L-mannofuranosyl)uracil

: 1453217-83-8
C₄₂H₄₆N₂O₈Si

Guidance literature:: With potassium carbonate; In methanol; at 23 ℃; for 1h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/jo401170y

Reference yield:

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1453217-83-8
C₄₂H₄₆N₂O₈Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium chlorochromate / dichloromethane / 13 h / 40 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -41 °C / Inert atmosphere

2.2: 2 h / -41 °C / Inert atmosphere

3.1: pyridine / 24 h / 110 °C / Inert atmosphere

4.1: acetic acid; water / 3 h / 90 °C

5.1: pyridine / 12 h / 23 °C / Inert atmosphere

6.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1 h / 90 °C / Inert atmosphere

6.2: 16 h / 0 - 50 °C / Inert atmosphere

7.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; boron trifluoride diethyl etherate; water; potassium carbonate; acetic acid; pyridinium chlorochromate; In methanol; dichloromethane; acetonitrile; 2.1: |Sakurai Allylation / 6.1: |Vorbrueggen Nucleoside Synthesis / 6.2: |Vorbrueggen Nucleoside Synthesis;
DOI:10.1021/jo401170y

Reference yield:

(3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde: (3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde

: 1453217-83-8
C₄₂H₄₆N₂O₈Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -41 °C / Inert atmosphere

1.2: 2 h / -41 °C / Inert atmosphere

2.1: pyridine / 24 h / 110 °C / Inert atmosphere

3.1: acetic acid; water / 3 h / 90 °C

4.1: pyridine / 12 h / 23 °C / Inert atmosphere

5.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1 h / 90 °C / Inert atmosphere

5.2: 16 h / 0 - 50 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; boron trifluoride diethyl etherate; water; potassium carbonate; acetic acid; In methanol; dichloromethane; acetonitrile; 1.1: |Sakurai Allylation / 5.1: |Vorbrueggen Nucleoside Synthesis / 5.2: |Vorbrueggen Nucleoside Synthesis;
DOI:10.1021/jo401170y