Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

Base Information

Chemical Name:Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2
CAS No.:350831-79-7
Molecular Formula:C₄₃H₄₅ClO₄OsP₂Si
Molecular Weight:941.514
Hs Code.:

Os(Si(OC<sub>2</sub>H<sub>5</sub>)3)Cl(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)2

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Chemical Property of Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

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Technology Process of Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

There total 2 articles about Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: OsCl(triphenylphosphine)2(CO)(Ph)

: 998-30-1
Triethoxysilane

: 350831-79-7
Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

Guidance literature:: In toluene; (N2); heating a mixt. of silicon compd. and osmium complex in toluene for 2 h; evapn., dissolving in CH2Cl2, filtration through Celite pad, addn. of EtOH, evapn., recrystn. (CH2Cl2/EtOH 25:10 vol.); elem. anal.;
DOI:10.1016/S0022-328X(00)00899-8

Reference yield:

: 350831-81-1
Os(Si(OC₂H₅)3)Cl(CO)2(P(C₆H₅)3)2

: 350831-79-7
Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

: 201230-82-2
carbon monoxide

Guidance literature:: In neat (no solvent, solid phase); heating osmium complex at 125°C in vac.;
DOI:10.1016/S0022-328X(00)00899-8

Reference yield: 90.0%

: 350831-79-7
Os(Si(OC₂H₅)3)Cl(CO)(P(C₆H₅)3)2

: 6699-93-0
(2-methylphenyl)lithium

: 350831-87-7
Os(Si(OC₂H₅)3)C₆H₄CH₃(CO)(P(C₆H₅)3)2

Guidance literature:: In diethyl ether; benzene; addn. of a soln. of CH3C6H4Li in Et2O to a soln. of osmium complex in C6H6 at 5°C, warming to room temp., stirring for 30 min; concn., addn. of hexane, filtration, washing with EtOH and hexane; elem.anal.;
DOI:10.1016/S0022-328X(00)00899-8