3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

Base Information

Chemical Name:3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose
CAS No.:100924-44-5
Molecular Formula:C₁₇H₂₃O₈P
Molecular Weight:386.339
Hs Code.:

3-O-Acetyl-1,2-O-isopropylidene-5-C-<methoxy(phenyl)phosphinyl>-α-D-xylopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

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Technology Process of 3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

There total 1 articles about 3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 7162-15-4,111469-75-1,121467-78-5
methyl phenylphosphinate

: 24807-97-4
3-O-acetyl-1,2-O-isopropylidene-α-D-xylo-pentodialdo-1,4-furanose

: 100924-44-5
3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

Guidance literature:: With triethylamine;
DOI:10.1016/S0008-6215(00)90466-X

Reference yield: 70.0%

: 100924-44-5
3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 100924-45-6
3-O-Acetyl-5-O-(imidazol-1-ylthiocarbonyl)-1,2-O-isopropylidene-5-C--α-D-xylofuranose

Guidance literature:: In 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)90466-X

Reference yield:

: 100924-44-5
3-O-Acetyl-1,2-O-isopropylidene-5-C--α-D-xylopyranose

: 100924-47-8
5-Deoxy-1,2-O-isopropylidene-5-C-(phenylphosphinyl)-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 1,2-dichloro-ethane

2: 90 percent / Tributyltin hydride / toluene / Heating

3: 84 percent / Sodium dihydrobis(2-methoxyethoxy)aluminate (SMDA) 70percent in benzene / tetrahydrofuran / 1 h / 0 °C

With tri-n-butyl-tin hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; 1,2-dichloro-ethane; toluene;
DOI:10.1016/S0008-6215(00)90466-X