<(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid

Base Information

Chemical Name:<(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid
CAS No.:148646-28-0
Molecular Formula:C₁₀H₁₂F₃O₂P
Molecular Weight:252.173
Hs Code.:

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Chemical Property of <(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid

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Technology Process of <(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid

There total 1 articles about <(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

: 434-45-7
2,2,2-Trifluoroacetophenone

: 7211-39-4
dimethyl phosphine oxide

: 148646-28-0
<(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid

Guidance literature:: In dichloromethane; for 12h; Ambient temperature;

Reference yield: 88.6%

: 109-63-7
trifluoroborane diethyl ether

: 148646-28-0
<(1-Hydroxy-1-phenyl-1-trifluormethyl)methyl>dimethylphosphinoxid

: 153048-16-9
(CH₃)2P(O)BF₃C(C₆H₅)(OH)CF₃

Guidance literature:: In dichloromethane; byproducts: Et2O; nitrogen atmosphere; B-compd. addn. (dropwise, 5 min) to org. compd. suspn., stirring (1 h, room temp.); solvent removal (vac.), residue recrystn. (dichloromethane/acetonitrile 1:1); elem. anal.;