C₆₆H₆₀

Base Information

Chemical Name:C₆₆H₆₀
CAS No.:1325730-14-0
Molecular Formula:C₆₆H₆₀
Molecular Weight:853.202
Hs Code.:

Synonyms:

Suppliers and Price of C₆₆H₆₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₆H₆₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₆H₆₀

There total 8 articles about C₆₆H₆₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 860435-39-8
2-bromo-4-tert-butyl-1-iodobenzene

: 1325730-14-0
C₆₆H₆₀

Guidance literature:: Multi-step reaction with 7 steps

1: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / diethylamine / 0 - 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 24 h / 80 °C / Inert atmosphere

3: Iodine monochloride / dichloromethane / 3 h / -78 °C / Inert atmosphere

4: trans-bis(triphenylphosphine)palladium dichloride; sodium carbonate / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere

5: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 6 h / 50 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / 80 °C / Inert atmosphere

7: potassium carbonate / methanol; dichloromethane / 3 h / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trans-bis(triphenylphosphine)palladium dichloride; Iodine monochloride; sodium carbonate; potassium carbonate; In methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl acetamide; water; diethylamine; N,N-dimethyl-formamide; toluene; 4: Mizoroki-Heck coupling reaction / 6: Suzuki coupling;
DOI:10.1021/ol201854g

Reference yield:

: 1325730-08-2
C₄₂H₃₆

: 1325730-14-0
C₆₆H₆₀

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / chloroform; N,N-dimethyl-formamide / 6 h / 50 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / 80 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 3 h / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; In methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; 2: Suzuki coupling;
DOI:10.1021/ol201854g

Reference yield:

: 1325730-13-9
C₄₂H₃₄Br₂

: 1325730-14-0
C₆₆H₆₀

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / 80 °C / Inert atmosphere

2: potassium carbonate / methanol; dichloromethane / 3 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; In methanol; ethanol; dichloromethane; water; toluene; 1: Suzuki coupling;
DOI:10.1021/ol201854g