2,4,6-trimethylphenyldibromogallate

Base Information

Chemical Name:2,4,6-trimethylphenyldibromogallate
CAS No.:154204-81-6
Molecular Formula:C₉H₁₁Br₂Ga
Molecular Weight:348.717
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4,6-trimethylphenyldibromogallate

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Technology Process of 2,4,6-trimethylphenyldibromogallate

There total 1 articles about 2,4,6-trimethylphenyldibromogallate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 13450-88-9
gallium(III) bromide

: 60607-12-7
trimesitylgallium

: 154204-81-6
2,4,6-trimethylphenyldibromogallate

Guidance literature:: In toluene; to a soln. of Mes3Ga GaBr3 is added, mixt. is refluxed for 10 h followed by stirring for 12 h at room temp.; ppt. is filtered off, washed several times with toluene, elem. anal.;

Reference yield: 81.0%

: 154204-81-6
2,4,6-trimethylphenyldibromogallate

: 113107-46-3
2,2-dimethyl-1,3-bis<(trimethylsilyl)amino>propane

: 164077-71-8
2-bromo-2-mesityl-5,5-dimethyl-1,3-bis(trimethylsilyl)-1-aza-3-azonia-2-gallatacyclohexane

Guidance literature:: With n-BuLi; In hexane; byproducts: LiBr; N2 atmosphere, addn. of soln. of n-BuLi to soln. of silyl compound (ratio = 1:1), addn. to suspension of Ga(C6H2(CH3)3Br2 at room temp., stirring (overnight); filtration, concn. (vacuum), crystn. (pentane, -78°C); elem. anal.;

Reference yield: 68.0%

: 154204-81-6
2,4,6-trimethylphenyldibromogallate

: 13400-13-0
cesium fluoride

: caesium 2,4,6-trimethylphenyltrifluorogallate

Guidance literature:: In acetonitrile; to a soln. of MesGaBr2 CsF is added, suspn. is stirred for 60 h at room temp.; hot suspn. is filtered, ppt. is crystd. from the filtrate, elem. anal.;