[1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride

Base Information

Chemical Name:[1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride
CAS No.:920281-53-4
Molecular Formula:C₁₈H₂₁Cl₃Ti
Molecular Weight:391.604
Hs Code.:

Synonyms:

Suppliers and Price of [1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride

There total 1 articles about [1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 3141-04-6
cyclopenta-2,4-dien-1-ylidenecyclohexane

: 7550-45-0
titanium tetrachloride

: 2417-95-0
p-tolyllithium

: 920281-53-4
[1-(4-methylphenyl)cyclohexyl]-cyclopentadienyl titanium trichloride

Guidance literature:: With chloro-trimethyl-silane; In tetrahydrofuran; diethyl ether; dichloromethane; under N2, Schlenk techniques; Li compd. in ice-cooled Et2O mixed with ligand (1:1), stirred for 12 h at room temp., filtered, washed (Et2O), dissolved (THF), (CH3)3SiCl (1.1 equiv.) added, evapd., triturated (CH2Cl2), cooled -20°C,TiCl4 (0.8 equ); stirred at room temp. for 12 h, evapd., extd. (hexane), crystd. on cooling to -30°C;
DOI:10.1016/j.molcata.2005.12.030