N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

Base Information

Chemical Name:N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate
CAS No.:1404194-11-1
Molecular Formula:C₁₇H₂₆N*FO₃S
Molecular Weight:343.463
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

Chemical Property:

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Technology Process of N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

There total 1 articles about N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 421-20-5
Methyl fluorosulfonate

: 101254-85-7
2,4,6-tri(isopropyl)benzonitrile

: 1404194-11-1
N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

Guidance literature:: at 45 ℃; for 45h;
DOI:10.1021/jo301983s

Reference yield:

: 1404194-11-1
N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

: 1404194-17-7
C₁₈H₂₉NO

Guidance literature:: Multi-step reaction with 2 steps

1: [D₃]acetonitrile / 0.08 h / -20 °C

2: methanol / dichloromethane / -78 °C

With methanol; In dichloromethane; [D₃]acetonitrile;
DOI:10.1021/jo301983s

Reference yield:

: 1404194-11-1
N-methyl-2,4,6-trisisopropylbenzonitrilium fluorosulfonate

: 1404194-18-8
C₁₈H₃₀NO⁽¹⁺⁾*FO₃S^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: [D₃]acetonitrile / 0.08 h / -20 °C

2: methanol / dichloromethane / -78 °C

3: [D₃]acetonitrile / 0.08 h / -20 °C

With methanol; In dichloromethane; [D₃]acetonitrile;
DOI:10.1021/jo301983s