C₃₅H₄₅ClN₄O₆S

Base Information

Chemical Name:C₃₅H₄₅ClN₄O₆S
CAS No.:1384259-14-6
Molecular Formula:C₃₅H₄₅ClN₄O₆S
Molecular Weight:685.284
Hs Code.:

C<sub>35</sub>H<sub>45</sub>ClN<sub>4</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₃₅H₄₅ClN₄O₆S

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Technology Process of C₃₅H₄₅ClN₄O₆S

There total 3 articles about C₃₅H₄₅ClN₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1384259-06-6
C₃₅H₄₄ClN₃O₄

: 1384259-14-6
C₃₅H₄₅ClN₄O₆S

Guidance literature:: With sulfonamide; In 1,2-dioxacyclohexane; at 100 ℃;
DOI:10.1016/j.bmcl.2012.04.113

Reference yield:

: 879498-90-5
1H-indole-6-carboxylic acid, 2-bromo-3-cyclohexyl-, 1,1-dimethylethyl ester

: 1384259-14-6
C₃₅H₄₅ClN₄O₆S

Guidance literature:: Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / 1,2-dimethoxyethane; water / 1 h / 70 °C

2: caesium carbonate / N,N-dimethyl-formamide / 60 °C

3: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

5: sulfonamide / 1,2-dioxacyclohexane / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; sulfonamide; water; potassium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; 1,2-dioxacyclohexane; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.113

Reference yield:

: 1204417-91-3
tert-butyl 3-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-6-carboxylate

: 1384259-14-6
C₃₅H₄₅ClN₄O₆S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 1 h / 70 °C

2: caesium carbonate / N,N-dimethyl-formamide / 60 °C

3: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

5: sulfonamide / 1,2-dioxacyclohexane / 100 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfonamide; water; sodium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; 1,2-dioxacyclohexane; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.113