[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]⁽¹⁺⁾*BF₄^(1-)=[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]BF₄

Base Information

• Chemical Name: [Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]⁽¹⁺⁾*BF₄^(1-)=[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]BF₄
• CAS No.: 155804-90-3
• Molecular Formula: BF₄*C₃₁H₂₇N₃O₃PPd
• Molecular Weight: 713.772
• Mol file: 155804-90-3.mol

Synonyms:

Chemical Property of [Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]⁽¹⁺⁾*BF₄^(1-)=[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]⁽¹⁺⁾*BF₄^(1-)=[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]BF₄

There total 3 articles about [Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]⁽¹⁺⁾*BF₄^(1-)=[Pd(P(OC₆H₅)3)(C₅NH₄C(CH₃)NNHC₆H₄)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

triphenyl phosphite (101-02-0) + thallium(I) tetrafluoroborate (28625-02-7) + [Pd(C6H4N(H)N=CMe(C5H4N))(Cl)] (155804-84-5) → [Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)](1+)*BF4(1-)=[Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)]BF4 (155804-90-3)

Guidance literature:

In acetone; to a suspn. of the Pd-complex in acetone is added P(OPh)3, after stirring for 5 min at room temp. is TlBF4 added, mixt is kept under stirring for 1 h; soln. is filtd., solvent is removed under vac., residue is treated withCH2Cl2 and filtd. again, addn. of hexane and concn., ppt. is washed with hexane and dried in vac., elem. anal.;

Reference yield:

[Pd(C6H5N(H)N=CMe(C5H4N))(Cl2)] (155804-82-3) → [Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)](1+)*BF4(1-)=[Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)]BF4 (155804-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: acetone

In acetone;

Reference yield:

2-acetylpyridine phenylhydrazone (7734-05-6) → [Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)](1+)*BF4(1-)=[Pd(P(OC6H5)3)(C5NH4C(CH3)NNHC6H4)]BF4 (155804-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol

2: acetone

3: acetone

In methanol; acetone;

upstream raw materials:

triphenyl phosphite

thallium(I) tetrafluoroborate

[Pd(C₆H₄N(H)N=CMe(C₅H₄N))(Cl)]

[Pd(C₆H₅N(H)N=CMe(C₅H₄N))(Cl₂)]

Refernces