2-Acetylpyridine phenylhydrazone

Base Information

• Chemical Name: 2-Acetylpyridine phenylhydrazone
• CAS No.: 7734-05-6
• Molecular Formula: C13H13N3
• Molecular Weight: 211.266
• European Community (EC) Number: 666-233-0
• DSSTox Substance ID: DTXSID20998571
• Mol file: 7734-05-6.mol

Synonyms:7734-05-6;1-(2-pyridinyl)-1-ethanone N-phenylhydrazone;2-ACETYLPYRIDINE PHENYLHYDRAZONE;DTXSID20998571;AKOS030240952;(E)-2-(1-(2-phenylhydrazono)ethyl)pyridine

Chemical Property of 2-Acetylpyridine phenylhydrazone

Chemical Property:

• Vapor Pressure: 4.09E-05mmHg at 25°C
• Boiling Point: 351.5°C at 760 mmHg
• Flash Point: 166.4°C
• PSA: 37.28000
• Density: 1.06g/cm³
• LogP: 2.99070
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 211.110947427
• Heavy Atom Count: 16
• Complexity: 231

Purity/Quality:

97% ^*data from raw suppliers

2-ACETYLPYRIDINE PHENYLHYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC1=CC=CC=C1)C2=CC=CC=N2

Technology Process of 2-Acetylpyridine phenylhydrazone

There total 2 articles about 2-Acetylpyridine phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-acetylpyridine (1122-62-9) + phenylhydrazine (100-63-0) → 2-acetylpyridine phenylhydrazone (7734-05-6)

Guidance literature:

In ethanol; at 50 ℃; for 1.5h;

DOI:10.1002/jhet.3130 DOI:10.1002/jhet.3251

Reference yield: 98.0%

2-acetylpyridine (1122-62-9) + phenylhydrazine hydrochloride (59-88-1) → 2-acetylpyridine phenylhydrazone (7734-05-6)

Guidance literature:

With sodium acetate; In ethanol; at 80 ℃; for 0.0833333h; Microwave irradiation; air-cooling;

DOI:10.1021/co100015b

Reference yield: 96.0%

2-acetylpyridine phenylhydrazone (7734-05-6) → 2-acetylpyridine (1122-62-9)

Guidance literature:

With Oxone; water; potassium hydrogencarbonate; In acetone; for 0.5h; Heating;

DOI:10.1080/00304949909355680

upstream raw materials:

2-acetylpyridine

phenylhydrazine

phenylhydrazine hydrochloride

Downstream raw materials:

2-acetylpyridine

phenylhydrazine

2-(piperidin-2-yl)-1H-indole

7-oxo-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizine