Iodomethyl p-Nitrophenyl Carbonate

Base Information

Chemical Name:Iodomethyl p-Nitrophenyl Carbonate
CAS No.:101623-71-6
Molecular Formula:C8H6INO5
Molecular Weight:323.044
Hs Code.:
DSSTox Substance ID:DTXSID601252492
Mol file:101623-71-6.mol

Synonyms:Iodomethyl p-Nitrophenyl Carbonate;101623-71-6;SCHEMBL25764;iodomethyl 4-nitrophenyl carbonate;NZKQUJFOPJXEFF-UHFFFAOYSA-N;DTXSID601252492;iodomethyl (4-nitrophenyl) carbonate;Carbonic acid, iodomethyl 4-nitrophenyl ester;carbonic acid iodomethyl ester 4-nitro-phenyl ester

Suppliers and Price of Iodomethyl p-Nitrophenyl Carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Iodomethyl p-Nitrophenyl Carbonate

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:322.92907
Heavy Atom Count:15
Complexity:234

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])OC(=O)OCI

Technology Process of Iodomethyl p-Nitrophenyl Carbonate

There total 5 articles about Iodomethyl p-Nitrophenyl Carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 50780-50-2
4-chloromethoxycarbonyloxy-1-nitrobenzene

: 101623-71-6
iodomethyl(4-nitrophenyl)carbonate

Guidance literature:: With sodium iodide; In acetone; at 50 ℃; for 24h;
DOI:10.1021/jo961696a

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 101623-71-6
iodomethyl(4-nitrophenyl)carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: morpholine / 1,2-dichloro-ethane / -78 - 20 °C / Inert atmosphere

2: sodium iodide / acetone / 24 h / Inert atmosphere; Reflux

With morpholine; sodium iodide; In 1,2-dichloro-ethane; acetone;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 101623-71-6
iodomethyl(4-nitrophenyl)carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / N-methylmorpholine / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, 24 h

2: 94 percent / NaI / acetone / 24 h / 50 °C

With 4-methyl-morpholine; sodium iodide; In chloroform; acetone;
DOI:10.1021/jo961696a