4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

Base Information

Chemical Name:4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate
CAS No.:1240485-63-5
Molecular Formula:C₁₃H₇NO₄S₅
Molecular Weight:401.533
Hs Code.:

Synonyms:

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Chemical Property of 4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

Chemical Property:

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Technology Process of 4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

There total 9 articles about 4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240485-62-4
4-nitrophenyl 2,2-dimethylbenzo[d][1,3,2]dithiastannole-5-carboxylate

: 1240485-63-5
4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

Guidance literature:: With disulfur dichloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo100870q

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 935687-90-4
3,4-disulfanylbenzoic acid

: 1240485-63-5
4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

Guidance literature:: 3,4-disulfanylbenzoic acid; With sodium hydroxide; In ethanol; at 20 ℃; for 0.25h;

With dimethyltin dichloride; In ethanol; water; at 20 ℃; for 1.5h;

4-nitro-phenol; Further stages;
DOI:10.1021/jo100870q

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1240485-61-3
2,2-dimethylbenzo[d][1,3,2]dithiastannole-5-carboxylic acid

: 1240485-63-5
4-nitrophenyl benzo[f]-[1,2,3,4,5]pentathiepine-7-carboxylate

Guidance literature:: 2,2-dimethylbenzo[d][1,3,2]dithiastannole-5-carboxylic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 0.166667h;

4-nitro-phenol; In dichloromethane;

With disulfur dichloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo100870q