Technology Process of C15H22INO2S2
There total 7 articles about C15H22INO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine;
In
tetrahydrofuran;
at 35 ℃;
for 0.5h;
optical yield given as %de;
diastereoselective reaction;
DOI:10.1021/co200129t
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C
4: iodine / tetrahydrofuran / 0.5 h / 35 °C
With
lithium aluminium tetrahydride; iodine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
DOI:10.1021/co200129t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C
2: iodine / tetrahydrofuran / 0.5 h / 35 °C
With
lithium aluminium tetrahydride; iodine;
In
tetrahydrofuran;
DOI:10.1021/co200129t