(2S,3R)-[2,3-²H]-α-tyrosine

Base Information

Chemical Name:(2S,3R)-[2,3-²H]-α-tyrosine
CAS No.:34100-65-7
Molecular Formula:C₉H₁₁NO₃
Molecular Weight:182.183
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-[2,3-²H]-α-tyrosine

Chemical Property:

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Technology Process of (2S,3R)-[2,3-²H]-α-tyrosine

There total 5 articles about (2S,3R)-[2,3-²H]-α-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-benzoyl-(2S,3R)-[3-²H]-tyrosine

: 34100-65-7
(2S,3R)-[2,3-²H]-α-tyrosine

Guidance literature:: N-benzoyl-(2S,3R)-[3-²H]-tyrosine; With hydrogen bromide; In water; for 3h; Reflux;

With acetic acid; sodium hydroxide; at 0 ℃; for 1h;
DOI:10.1021/ja403918w

Reference yield:

: 95307-64-5
4-hydroxybenzaldehyde

: 34100-65-7
(2S,3R)-[2,3-²H]-α-tyrosine

Guidance literature:: Multi-step reaction with 4 steps

1.1: dipotassium hydrogenphosphate; acetic anhydride / 80 °C / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: sodium hydroxide; water / ethanol / Reflux

3.1: [Rh(NBD)((R)-Prophos)]ClO₄; hydrogen / tetrahydrofuran / 16 h / 1500.15 Torr

3.2: Dowex 50 W (100?200 mesh) cation exchange resin

4.1: hydrogen bromide / water / 3 h / Reflux

4.2: 1 h / 0 °C

With dipotassium hydrogenphosphate; [Rh(NBD)((R)-Prophos)]ClO₄; water; hydrogen bromide; hydrogen; acetic anhydride; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja403918w

Reference yield:

: 1448510-72-2
(Z)-2-benzamido-[3-²H]-3-(4-hydroxyphenyl)acrylic acid

: 34100-65-7
(2S,3R)-[2,3-²H]-α-tyrosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: [Rh(NBD)((R)-Prophos)]ClO₄; hydrogen / tetrahydrofuran / 16 h / 1500.15 Torr

1.2: Dowex 50 W (100?200 mesh) cation exchange resin

2.1: hydrogen bromide / water / 3 h / Reflux

2.2: 1 h / 0 °C

With [Rh(NBD)((R)-Prophos)]ClO₄; hydrogen bromide; hydrogen; In tetrahydrofuran; water;
DOI:10.1021/ja403918w