Technology Process of C23H28N4O3S
There total 3 articles about C23H28N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 0.75 h / 60 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; toluene
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
ethanol; toluene;
DOI:10.1016/j.bmcl.2012.04.075
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / tetrahydrofuran; water / 2 h / 60 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 0.75 h / 60 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; toluene
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bmcl.2012.04.075
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; toluene;
DOI:10.1016/j.bmcl.2012.04.075