C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

Base Information

Chemical Name:C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾
CAS No.:1429768-22-8
Molecular Formula:C₃₀H₃₅N₆O₈S*Gd
Molecular Weight:796.959
Hs Code.:

C<sub>30</sub>H<sub>35</sub>N<sub>6</sub>O<sub>8</sub>S<sup>(3-)</sup>*Gd<sup>(3+)</sup>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

Chemical Property:

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Technology Process of C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

There total 9 articles about C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429762-69-5
2-(4’-chloroacetamide-phenyl)-6-metoxybenzothiazol-DO3A

: 1429768-22-8
C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

Guidance literature:: With gadolinium(III) chloride; sodium hydroxide; In water; at 59.84 ℃; for 24h; pH=7;
DOI:10.1021/ml400042w

Reference yield:

: 1429762-67-3
2-(4’-chloroacetamide-phenyl)-6-metoxybenzothiazol-tBu3DO3A

: 1429768-22-8
C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 45 °C

2: sodium hydroxide; gadolinium(III) chloride / water / 24 h / 59.84 °C / pH 7

With gadolinium(III) chloride; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/ml400042w

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1429768-22-8
C₃₀H₃₅N₆O₈S^(3-)*Gd⁽³⁺⁾

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

2: Lawessons reagent / chlorobenzene / 4 h / Reflux

3: sodium hydroxide / water; ethanol / 3 h / Reflux

4: tin(ll) chloride / ethanol / 4 h / Reflux

5: potassium carbonate / acetonitrile / 2 h

6: potassium carbonate / acetonitrile / 48 h / 20 °C

7: trifluoroacetic acid / dichloromethane / 45 °C

8: sodium hydroxide; gadolinium(III) chloride / water / 24 h / 59.84 °C / pH 7

With Lawessons reagent; gadolinium(III) chloride; potassium carbonate; triethylamine; trifluoroacetic acid; tin(ll) chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; chlorobenzene; acetonitrile;
DOI:10.1021/ml400042w