2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

Base Information

Chemical Name:2-(4-Chlorphenylthio)-4-nitrobenzylalkohol
CAS No.:66949-32-4
Molecular Formula:C₁₃H₁₀ClNO₃S
Molecular Weight:295.746
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

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Technology Process of 2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

There total 3 articles about 2-(4-Chlorphenylthio)-4-nitrobenzylalkohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66949-30-2
2-(4-chloro-phenylsulfanyl)-4-nitro-benzoic acid

: 66949-32-4
2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

Guidance literature:: With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran;
DOI:10.1135/cccc19780471

Reference yield:

: 16426-64-5
2-bromo-4-nitrobenzoic acid

: 66949-32-4
2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, Cu / hexamethylphosphoric acid triamide / 170 °C

2: NaBH₄, BF₃-Et₂O / tetrahydrofuran

With sodium tetrahydroborate; boron trifluoride diethyl etherate; copper; potassium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1135/cccc19780471

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 66949-32-4
2-(4-Chlorphenylthio)-4-nitrobenzylalkohol

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, Cu / hexamethylphosphoric acid triamide / 170 °C

2: NaBH₄, BF₃-Et₂O / tetrahydrofuran

With sodium tetrahydroborate; boron trifluoride diethyl etherate; copper; potassium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1135/cccc19780471