6-(3,3-dimethylallyl)alloptaeroxylin

Base Information

• Chemical Name: 6-(3,3-dimethylallyl)alloptaeroxylin
• CAS No.: 41440-04-4
• Molecular Formula: C₂₀H₂₂O₄
• Molecular Weight: 326.392

Synonyms:

Chemical Property of 6-(3,3-dimethylallyl)alloptaeroxylin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-(3,3-dimethylallyl)alloptaeroxylin

There total 2 articles about 6-(3,3-dimethylallyl)alloptaeroxylin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pulverin (24672-78-4) → 10-(3,3-dimethylallyl)spatheliachromene (33845-34-0) + 6-(3,3-dimethylallyl)alloptaeroxylin (41440-04-4)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 6h; Heating;

Reference yield:

pulverin (24672-78-4) → spatheliabischromene (34411-93-3) + 10-(3,3-dimethylallyl)spatheliachromene (33845-34-0) + 6-(3,3-dimethylallyl)alloptaeroxylin (41440-04-4)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 70h; Heating;

Reference yield:

6-(3,3-dimethylallyl)alloptaeroxylin (41440-04-4) → spatheliabischromene (34411-93-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 160 mg / conc. HCl / acetic acid / 1 h / Heating

2: 1.) NBS, dibenzoylperoxide 2.) pyridine / 1.) carbon tetrachloride, 3 h reflux 2.) 2h reflux or DDQ, benzene

With pyridine; hydrogenchloride; N-Bromosuccinimide; dibenzoyl peroxide; In acetic acid;

upstream raw materials:

pulverin

Downstream raw materials:

spatheliabischromene

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