Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate

Base Information

Chemical Name:Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate
CAS No.:1246936-63-9
Molecular Formula:C₃₂H₃₄N₂O₈PS*Li
Molecular Weight:644.611
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate

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Technology Process of Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate

There total 2 articles about Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112514-65-5
5'-O-(dimethoxytrityl)thymidine 3'-O-(2''-cyanoethylmethylphosphonothioate)

: 1246936-63-9
Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate

Guidance literature:: With ammonium hydroxide; Dowex Li+; In ethanol;
DOI:10.1016/S0040-4039(00)94646-X

Reference yield:

: 115393-52-7
5'-O-dimethoxytritylthymidine-3'-O-β-cyanoethoxymethylphosphonite

: 1246936-63-9
Li 5'-Dimethoxytritylthymidyl-3'-methylphosphonothioate

Guidance literature:: Multi-step reaction with 2 steps

1: S₈

2: 1) NH₄OH 2) Dowex Li+ / ethanol

With sulfur; ammonium hydroxide; Dowex Li+; In ethanol;
DOI:10.1016/S0040-4039(00)94646-X