(E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

Base Information

Chemical Name:(E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene
CAS No.:128292-92-2
Molecular Formula:C₁₄H₁₈O₂S
Molecular Weight:250.362
Hs Code.:

Synonyms:

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Chemical Property of (E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

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Technology Process of (E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

There total 4 articles about (E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149847-13-2
(2E)-2,5-dimethyl-2,4-hexadienal

: 128292-92-2
(E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.08 h / Ambient temperature

2: glac. AcOH / propan-2-ol / Heating

With lithium aluminium tetrahydride; acetic acid; In diethyl ether; isopropyl alcohol;
DOI:10.1039/P19930000987

Reference yield:

: 62285-97-6
4,4-dimethoxy-3-methyl-but-2-en-1-al

: 128292-92-2
(E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 1) BuLi / 1) Et₂O, hexane, r.t., 30 min, 2) Et₂O, hexane, r.t., 30 min

2: 15percent H₂SO₄ / acetone / 0.25 h / 0 °C

3: LiAlH₄ / diethyl ether / 0.08 h / Ambient temperature

4: glac. AcOH / propan-2-ol / Heating

With lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; acetic acid; In diethyl ether; isopropyl alcohol; acetone;
DOI:10.1039/P19930000987

Reference yield:

: 1026317-99-6
(E)-1,1-Dimethoxy-2,5-dimethyl-hexa-2,4-diene

: 128292-92-2
(E)-(2,5-Dimethylhexa-2,4-dienyl)sulfonylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 15percent H₂SO₄ / acetone / 0.25 h / 0 °C

2: LiAlH₄ / diethyl ether / 0.08 h / Ambient temperature

3: glac. AcOH / propan-2-ol / Heating

With lithium aluminium tetrahydride; sulfuric acid; acetic acid; In diethyl ether; isopropyl alcohol; acetone;
DOI:10.1039/P19930000987