rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid

Base Information

Chemical Name:rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid
CAS No.:1075278-52-2
Molecular Formula:C₂₄H₂₆F₄N₄O₆S₂
Molecular Weight:606.619
Hs Code.:

rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid

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Chemical Property of rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid

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Technology Process of rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid

There total 1 articles about rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10553-78-3
(acetylthio)acetyl chloride

: 1075221-43-0
rac-ethyl 3-amino-3-[4-(aminomethyl)phenyl]-2,2-difluoropropanoate hydrochloride

: 24424-99-5
di-tert-butyl dicarbonate

: 1075221-76-9
rac-3-amino-3-[4-(aminomethyl)phenyl]-2,2-difluoropropionic acid hydrochloride

: 1075278-52-2
rac-3-[4-(aminomethyl)phenyl]-3-[({[({1-[4-(aminomethyl)phenyl]-2-carboxy-2,2-difluoroethyl}carbamoyl)methyl]disulfanyl}acetyl)amino]-2,2-difluoropropionic acid

Guidance literature:: rac-ethyl 3-amino-3-[4-(aminomethyl)phenyl]-2,2-difluoropropanoate hydrochloride; di-tert-butyl dicarbonate; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 24h;

(acetylthio)acetyl chloride; With methanol; dmap; In dichloromethane; at 20 ℃; for 12h; Further stages; Inert atmosphere;
DOI:10.1002/ejoc.200800363