[Fe(CO)4(CNC₆H₁₁)]

Base Information

Chemical Name:[Fe(CO)4(CNC₆H₁₁)]
CAS No.:19706-02-6
Molecular Formula:C₁₁H₁₁FeNO₄
Molecular Weight:277.06
Hs Code.:

[Fe(CO)4(CNC<sub>6</sub>H<sub>11</sub>)]

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Chemical Property of [Fe(CO)4(CNC₆H₁₁)]

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Technology Process of [Fe(CO)4(CNC₆H₁₁)]

There total 5 articles about [Fe(CO)4(CNC₆H₁₁)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 108-91-8,157973-60-9
cyclohexylamine

: 19706-02-6,34871-29-9
[Fe(CO)4(CNC₆H₁₁)]

Guidance literature:: With n-butyllithium; Chloro-oxo-acetic acid; In tetrahydrofuran; under Ar; nBuLi added to soln. of amine in THF at -80°C, after 30min mixt. warmed to -10°C, soln. of Fe(CO)5 in THF added dropwis e, after 30 min mixt. cooled to -30°C, oxalylchloride added, stirred for 1 h; evapd. to dryness, amine sepd. by extracting residue with hexane at -40°C, residue extd. with hexane at 0°C, crystn. after 1 d at -30°C; elem. anal.;
DOI:10.1016/S0020-1693(02)01553-0

Reference yield: 10.0%

: 538-75-0
dicyclohexyl-carbodiimide

: 100447-70-9
triiron dodecacarbonyl

: 25792-38-5
Fe(CO)3(CNC₆H₁₁)2

: 19706-02-6,34871-29-9
Fe(CO)4(CNC₆H₁₁)

: 82044-62-0
[Fe2(CO)6(μ,μ'-(C6H11N)2CFe(CO)4)]

: 34871-26-6
[Fe2(CO)6(μ,μ'-(C6H11N)2CNC6H11)]

Guidance literature:: In n-heptane; under N2, soln. of Fe complex and dicyclohexylcarbodiimide in heptane heated to reflux until green color disappeared; filtered, solvent removed under reduced pressure, residue redissolved in hexane, chromd., recrystd. from hexane, elem. anal.;

Reference yield: 5.0%

: 15321-51-4
di-iron nonacarbonyl

: 538-75-0
dicyclohexyl-carbodiimide

: 19706-02-6,34871-29-9
Fe(CO)4(CNC₆H₁₁)

: 34871-26-6
[Fe2(CO)6(μ,μ'-(C6H11N)2CNC6H11)]

Guidance literature:: In hexane; under N2, mixt. of Fe complex and dicyclohexylcarbodiimide in hexane heated to reflux until Fe complex dissolved; solvent removed under reduced pressure, residue dissolved in benzene, chromd. on alumina, elem. anal.;