Technology Process of 4,4'''-Dimethoxy-2,2'''-dimethyl-2',2'',4''-trinitro-[1,3';1',1'';3'',1''']quaterphenyl-4'-ol
There total 4 articles about 4,4'''-Dimethoxy-2,2'''-dimethyl-2',2'',4''-trinitro-[1,3';1',1'';3'',1''']quaterphenyl-4'-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 14.07 g / copper(I) chloride/potassium t-butoxide, pyridine / 1,2-dimethoxy-ethane / 16 h / 80 °C
2: sodium benzaldehyde oxime / hexamethylphosphoric acid triamide
With
pyridine; potassium tert-butylate; benzaldoxime sodium salt; copper(l) chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 14.07 g / copper(I) chloride/potassium t-butoxide, pyridine / 1,2-dimethoxy-ethane / 16 h / 80 °C
2: sodium benzaldehyde oxime / hexamethylphosphoric acid triamide
With
pyridine; potassium tert-butylate; benzaldoxime sodium salt; copper(l) chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 g / iodine/periodic acid dihydrate / H2O; acetic acid; H2SO4 / 6 h
2: 14.07 g / copper(I) chloride/potassium t-butoxide, pyridine / 1,2-dimethoxy-ethane / 16 h / 80 °C
3: sodium benzaldehyde oxime / hexamethylphosphoric acid triamide
With
pyridine; potassium tert-butylate; iodine; benzaldoxime sodium salt; periodic acid; copper(l) chloride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; sulfuric acid; water; acetic acid;
