9-(p-hydroxyphenyl)-9-phenylselenoxanthene

Base Information

• Chemical Name: 9-(p-hydroxyphenyl)-9-phenylselenoxanthene
• CAS No.: 116905-84-1
• Molecular Formula: C₂₅H₁₈OSe
• Molecular Weight: 413.377
• Mol file: 116905-84-1.mol

Synonyms:

Chemical Property of 9-(p-hydroxyphenyl)-9-phenylselenoxanthene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(p-hydroxyphenyl)-9-phenylselenoxanthene

There total 3 articles about 9-(p-hydroxyphenyl)-9-phenylselenoxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C44H30OSe2 (116905-83-0) → 9-phenylselenoxanthenol (30571-10-9) + 9-(p-hydroxyphenyl)-9-phenylselenoxanthene (116905-84-1)

Guidance literature:

With hydrogenchloride; In benzene; for 5h; Heating;

DOI:10.1039/P19880002271

Reference yield:

phenol (108-95-2,27073-41-2) → 9-(p-hydroxyphenyl)-9-phenylselenoxanthene (116905-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) CH₃CN, 2.) CH₃CN, 1 h room t.

2: 83 percent / HCl gas / benzene / 5 h / Heating

With hydrogenchloride; sodium hydride; In benzene;

DOI:10.1039/P19880002271

Reference yield:

9-phenylselenoxanthylium perchlorate + phenol (108-95-2,27073-41-2) → 9-(p-hydroxyphenyl)-9-phenylselenoxanthene (116905-84-1)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) 50 deg C, 2.) 1 h, 50 deg c;

DOI:10.1039/P19880002271

upstream raw materials:

C₄₄H₃₀OSe₂

phenol

Downstream raw materials:

9-(p-methoxyphenyl)-9-phenylselenoxanthene

Refernces