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(CO)3FeFe(CO)3((C6H5)2CCN(C6H5))

Base Information
  • Chemical Name:(CO)3FeFe(CO)3((C6H5)2CCN(C6H5))
  • CAS No.:112312-24-0
  • Molecular Formula:C26H15Fe2NO6
  • Molecular Weight:549.102
  • Hs Code.:
(CO)3FeFe(CO)3((C<sub>6</sub>H<sub>5</sub>)2CCN(C<sub>6</sub>H<sub>5</sub>))

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Chemical Property of (CO)3FeFe(CO)3((C6H5)2CCN(C6H5))
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Technology Process of (CO)3FeFe(CO)3((C6H5)2CCN(C6H5))

There total 3 articles about (CO)3FeFe(CO)3((C6H5)2CCN(C6H5)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; Irradiation (UV/VIS); soln. of ketenimine and Fe(CO)5 in toluene was irradiated with 125W Hg high-pressure lamp for 24 h under N2; evapd., residue was taken up in toluene, chromd. over Kieselgel (eluenttoluene for Fe-complex followed by CH2Cl2 for imidazolidinone), eluateswere evapd., Fe-complex was recrystd. from pentane at -20°C, imidazolidinone - from heptane;
DOI:10.1016/0022-328X(87)85008-8
Guidance literature:
In pentane; byproducts: Fe3(CO)12; suspn. of ketenimine and Fe-complex in pentane was stirred under N2 at room temp. for 48 h; filtered, washed with pentane, concd., chromd. over Kieselgel (eluates petroleum ether (p.e.) for Fe3(CO)12, p.e.-toluene for azaallyl complex (elem. anal.), toluene for ferrole), Fe-complexes recrystd. from pentane, imidazolidinone was extd. from ppt.;
DOI:10.1016/0022-328X(87)85008-8
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