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Technology Process of Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6

Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6

Base Information
  • Chemical Name:Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6
  • CAS No.:331990-35-3
  • Molecular Formula:C32H54P2Rh*F6P
  • Molecular Weight:748.598
  • Hs Code.:
Rh(C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Rh(C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)2PF<sub>6</sub>

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Chemical Property of Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6
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Technology Process of Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6

There total 1 articles about Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

silver(I) hexafluorophosphate
26042-63-7

silver(I) hexafluorophosphate

C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2P(C<sub>4</sub>H<sub>9</sub>)2C<sub>2</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>RhHCl

C6H5C2H4P(C4H9)2P(C4H9)2C2H4C6H4RhHCl

RhH(C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)(C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)<sup>(1+)</sup>

RhH(C6H5C2H4P(C4H9)2)(C6H4C2H4P(C4H9)2)(1+)

Rh(C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Rh(C<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>P(C<sub>4</sub>H<sub>9</sub>)2)2PF<sub>6</sub>
331990-35-3

Rh(C6H5C2H4P(C4H9)2)2(1+)*PF6(1-)=Rh(C6H5C2H4P(C4H9)2)2PF6

Guidance literature:
In diethyl ether; toluene; byproducts: AlCl; a soln. of complex in toluene was treated at -60°C with a soln. of AgPF6 in ether, warmed to room temp.; filtered, the filtrate was evapd. in vac., the residue was extd. with CH2Cl2, evapd. to dryness, dissolved in acetone, ether was added with stirring, the solid was washed with ether and pentane, dried;
DOI:10.1021/om0010159
upstream raw materials:

silver(I) hexafluorophosphate

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