Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester

Base Information

• Chemical Name: Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester
• CAS No.: 170999-49-2
• Molecular Formula: C₁₇H₁₉N₂O₉PS
• Molecular Weight: 458.386

Synonyms:

Chemical Property of Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester

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Technology Process of Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester

There total 2 articles about Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ⁵-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Di-imidazol-1-yl-phosphinic acid (2R,3S,5R)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester (170999-47-0) → Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester (170999-49-2)

Guidance literature:

Multi-step reaction with 3 steps

1: acetonitrile / 1 h / Ambient temperature

2: Cl₂CHCO₂H / CH₂Cl₂ / 0.02 h

3: N-methylimidazole / acetonitrile / 1 h / Ambient temperature

With 1-methyl-1H-imidazole; dichloro-acetic acid; In dichloromethane; acetonitrile;

Reference yield:

C45H45N2O14PS2 → Toluene-4-sulfonic acid (4aR,6R,7aS)-6-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-oxo-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinin-2-yl ester (170999-49-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Cl₂CHCO₂H / CH₂Cl₂ / 0.02 h

2: N-methylimidazole / acetonitrile / 1 h / Ambient temperature

With 1-methyl-1H-imidazole; dichloro-acetic acid; In dichloromethane; acetonitrile;

upstream raw materials:

Di-imidazol-1-yl-phosphinic acid (2R,3S,5R)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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