C₁₈H₂₄O₂

Base Information

Chemical Name:C₁₈H₂₄O₂
CAS No.:133663-83-9
Molecular Formula:C₁₈H₂₄O₂
Molecular Weight:272.387
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₄O₂

Chemical Property:

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Technology Process of C₁₈H₂₄O₂

There total 17 articles about C₁₈H₂₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 100-39-0
benzyl bromide

: 85757-79-5
C₁₁H₁₈O₂

: 133663-83-9
C₁₈H₂₄O₂

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3230

Reference yield:

: 133663-79-3
methyl (S)-3-oxo-4-(2-cyclopentenyl)butyrate

: 133663-83-9
C₁₈H₂₄O₂

Guidance literature:: Multi-step reaction with 10 steps

1: p-toluenesulfonyl azide, NEt₃ / acetonitrile / 12 h / 20 °C

2: copper(II) acetylacetonate / toluene / 2 h / Heating

3: 78 percent / conc. H₂SO₄, HOAc / 2 h / 20 °C

4: conc. H₂SO₄, HOAc / 0.5 h / Heating

5: K₂CO₃ / methanol / 2 h / 20 °C

6: diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 14 h / Ambient temperature

7: K₂CO₃ / methanol / 2 h / 20 °C

8: 1.) lithium diethylamide / 1.) THF, toluene, 0 deg C, 10 min, 2.) 0.5 h

9: 1 percent / Zn-Cu, I₂ / diethyl ether / 1 h / Heating

10: 50 percent / NaH / dimethylformamide

With 4-toluenesulfonyl azide; sulfuric acid; lithium diethylamide; iodine; copper; sodium hydride; potassium carbonate; acetic acid; triethylamine; triphenylphosphine; zinc; diethylazodicarboxylate; copper acetylacetonate; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1248/cpb.38.3230

Reference yield:

: 85757-74-0
(1R,5R,6S)-6-benzyloxy-cis-bicyclo<3.3.0>octan-3-one

: 133663-83-9
C₁₈H₂₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / 5percent Pd-C / methanol / 16 h / Ambient temperature

2: 1.) lithium diethylamide / 1.) THF, toluene, 0 deg C, 10 min, 2.) 0.5 h

3: 1 percent / Zn-Cu, I₂ / diethyl ether / 1 h / Heating

4: 50 percent / NaH / dimethylformamide

With lithium diethylamide; hydrogen; iodine; copper; sodium hydride; zinc; palladium on activated charcoal; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3230